Stage 1 -
Pre-Acid Cleaning Preparation
Choose the
method of circulation. Install the acid circulating pump and hoses
accordingly.
Fill the
equipment up with water to flood the entire surface to be cleaned.
If you have a
way to heat up the water to about 140°F, do so. This will enhance the
acid reaction with lime. The additional heat will also aid in the
circulation.
Stage 2 - Acid
Cleaning
Calculate the
water capacity of the system.
Pump 5% - 10% of
this capacity in acid. If the system holds 1000 gallons of water, add 50
- 100 gallons of acid. pH of the initial solution should be around 1.0.
Remember the old
chemistry rule: Add acid into water (not water into acid). The latter
will cause a violent reaction and can result in injury.
Start the acid
circulation pump to circulate the acid solution through the equipment.
Check pH
immediately. pH must start at about 1.0. If pH is higher, pump
additional acid into the equipment until pH drops to about 1.0.
Check pH every
hour. As pH increases to about 2.0, add additional acid to drop the pH
back to 1.0.
Once pH
stabilizes at about 1.5 for 2 hours, it indicates that no additional
scale is being removed. As such, it usually indicates that the removal
of the scale is completed.
Depending on the
quantity of scale to be removed, acid cleaning time can take up to 24
hours. Typically, circulation of 8 - 12 hours is sufficient.
When the
equipment is cleaned sufficiently, stop the acid circulation pump.
Dispose,
Neutralize, or Treat the acid solution, as discussed in the Acid
Cleaning Hazards - Proper Planning and Preparation Guidelines.
To neutralize,
you may do this while the acid is in the equipment so you don’t have
to use another tank. You will form sludge in the equipment but they can
be flushed out by pressure washing. Add caustic slowly to raise the pH
to the desired level.
Drain the
treated acid solution out of the equipment.
Stage 3 - Post
Acid Cleaning Guidelines
Flush the
equipment thoroughly with fresh water. Continue flushing until all the
loose particles are flushed out. Pressure washing will help.
Inspect the
internal to see if the scale removal is sufficient. Inspect for any
damage too, so repairs can be made before placing the equipment back in
service.
Remove all caps.
You may need to physically clean these capped nipples, as these areas
have a tendency to collect particles during the acid cleaning process,
due to poor circulation.
Install all the
piping that were removed during Stage 1.
Start-up or
pressure test the equipment for leaks.
Immediately
refill the equipment with treated water to prevent flash corrosion and
possible residual acid in crevices. Final pH must not be acidic.